For example, replacing septa or liner at regular intervals and keeping the injector and detector clean and well-maintained shoud solve many problems. More Buying Choices 320.61 (2 used & new offers)The new ENGEL e-mac: compact on the outside, huge on the inside We have made our e-mac series even more compact, allowing you to optimally utilise your production floor space: a significantly shorter clamping unit of course with the same maximum opening stroke and a smaller footprint on the non-operator side make the new e-mac the machine with the smallest footprint in its class.Many GC problems can be prevented if the column is properly installed and GC is maintained routinely. Get it as soon as Thu, Sep 30. 5 coupon applied at checkout Save 5 with coupon. They also offer a line of custom stainless steel moldings for running boards, hoods, body trim and interior trim.» Chromatography » Hints and tips » GC troubleshooting » GC troubleshooting GC troubleshooting PreventionAUTOOL Ultrasonic Fuel Injector Cleaner Tester Support Petrol Motorcycle Automotive Fuel Cleaning. The product line consists of nerf bars, chin bars, bumpers, air cleaner covers, multi stack fuel injection look air cleaners, faux fuel injection, low profile fuel injection look air cleaners and side vents.During this time the injectors are opened and. With the proper fuel injector cleaning equipment and chemicals it takes the professionals about 45 60 minutes of actual cleaning time to clean a single or set of fuel injectors. It can clean several injectors and.DIY’ers do not have the proper equipment to test, measure, verify and clean the internals of the fuel injectors.Spiking is presented by peaks with no width, either positive or negativeDownward drift for a few minutes is normal after installing a new columnIncrease the oven temperature to close to the maximum continuous operating temperature for the column. Offset is sudden unexplained change of the baseline position Noise is rapid and random movement of the baseline position Drift means slow baseline movement in one direction Baseline problemsBaseline problems could be divided into 5 categories: drift, noise, offset, spiking and wander. Its clean user interface offers a set of basic parameters that can be.For the problem identification we recommend to use electronic flowmeter and leak detector.
Injector Cleaner Hine Mac Series Even![]() If it does not help, replace the column.Monitor line voltage for correlation with offset. Cut off first 10 cm of column. Replace inlet liner, septa and selas.Bake out the column. If necessary, install a voltage regulator.Baseline wandering may be caused by changes in environmental conditions such as temperature or line voltageTry to correlate the wandering with environmental parameters. Turn off equipment or move it. Periodicity is often a clue. Clean any dirty or corroded connections.Column inserted too fat into the flame of FID, NPD or FPD detectorsElectrical disturbances entering the chromatograph through power cables, even shielded cablesTry to correlate spikes with events in equipment near the chromatograph. Tighten any loose connections. Solutions include reducing the injection volume or using a column with greatr capacity. In this case, the effect should be a function of injection volume. The peaks are clipped with flat tops.Attenuate detector output or reduce sample amount (see above).Fronting peaks are usually the result of column overloading. The broad peaks may have a rounded top or even valleys in the top.Reduce sample volume, dilute with solvent or use higher split ratio.Overload of the signal processing electronics. Replace inlet liner, glass wool and seals.Distorted peak shapes All peaks redused in size Possible causeCheck the concentration and stability of the sample.Detector overload. Condition the column at temperature higher than has been used but lower than the maximum continuous operation temperature for the column. If ghost peaks continue to occur, clean the inlet. Ghost peaks due to remmants are most likely to occur when increasing inlet or column temperatures.Increase the final temperature and lengthen the run time to allow for complete elution of previous samples. Ghost peaks Possible causeRemmants of previous samples in the inlet or column. Replace the inlet liner, glass wool and seals.Irreproducible peak heights or areas Possible causeDevelop a reproducible injection technique. These condensates may vaporize later and interfere with subsequent analyses, sometimes producing "ghost peaks".Bleed from the septum or fragments of the septum lodged in the inlet or liner.Clean the inlet. Less volatile components may condense. These vapours may come in contact with colder spots, such as the septum and gas inlets of the injector. Backflash refers to vapours from the sample which expand to exceed the volume of the injector liner. If it does not help, replace the column.Backflash may cause remmants. ![]() Later eluting and less volatile compounds have low response.Mixed sample solvent for splitless or on-column injectionsWhen using injection techniques that require " solvent effect" refocusing such as splitless injectiion, the solvent must form a compact, continuous flooded zone in the column. Injector temperature is too low. Decrease the initial column temperature or use less volatile solvent.Inlet descrimination. This affects the more volatile components most.Initial column temperature should be below the boiling point of the solvent. Bake out the column or replace it.Injector leaks reduce the peak height of the most volatile components of a sample more than less volatileInitial column temperature too high for splitless injection which can prevent refocusing of sample. Olm to pst converter for macThis will result in broad and distorted peaks because the solutes will not be refocused into a narrow band near the beginning of the column.
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